N-(4-methoxyphenyl)-4-phenoxybenzamide

Base Information

Chemical Name:N-(4-methoxyphenyl)-4-phenoxybenzamide
CAS No.:723255-63-8
Molecular Formula:C₂₀H₁₇NO₃
Molecular Weight:319.36
Hs Code.:
Mol file:723255-63-8.mol

Synonyms:

Suppliers and Price of N-(4-methoxyphenyl)-4-phenoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(4-methoxyphenyl)-4-phenoxybenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(4-methoxyphenyl)-4-phenoxybenzamide

There total 3 articles about N-(4-methoxyphenyl)-4-phenoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-50-4
iodobenzene

: 723255-63-8
N-(4-methoxyphenyl)-4-phenoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / 90 °C / Inert atmosphere

2: sodium hydroxide; water / ethanol / 3 h / Reflux

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine; triethylamine / dichloromethane / 0 - 20 °C

With 4-methyl-morpholine; copper(l) iodide; dimethylaminoacetic acid; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In 1,4-dioxane; ethanol; dichloromethane; 1: |Ullmann Condensation;
DOI:10.1007/s12272-015-0578-7

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 723255-63-8
N-(4-methoxyphenyl)-4-phenoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / 90 °C / Inert atmosphere

2: sodium hydroxide; water / ethanol / 3 h / Reflux

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine; triethylamine / dichloromethane / 0 - 20 °C

With 4-methyl-morpholine; copper(l) iodide; dimethylaminoacetic acid; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In 1,4-dioxane; ethanol; dichloromethane; 1: |Ullmann Condensation;
DOI:10.1007/s12272-015-0578-7

Reference yield:

: 31994-68-0
4-phenoxybenzoic acid ethyl ester

: 723255-63-8
N-(4-methoxyphenyl)-4-phenoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / ethanol / 3 h / Reflux

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine; triethylamine / dichloromethane / 0 - 20 °C

With 4-methyl-morpholine; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1007/s12272-015-0578-7