bis(1-azepanylmethyl)phosphinic acid

Base Information

• Chemical Name: bis(1-azepanylmethyl)phosphinic acid
• CAS No.: 244201-57-8
• Molecular Formula: C₁₄H₂₉N₂O₂P
• Molecular Weight: 288.37
• Mol file: 244201-57-8.mol

Synonyms:

Chemical Property of bis(1-azepanylmethyl)phosphinic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of bis(1-azepanylmethyl)phosphinic acid

There total 2 articles about bis(1-azepanylmethyl)phosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

trimethylsilyl bis(N-methyl-N-formylaminomethyl)phosphinate → bis(perhydroazepinomethyl)phosphinic acid (244201-57-8)

Guidance literature:

With methanol; In diethyl ether; at 10 ℃; for 1h; Inert atmosphere; Heating;

DOI:10.1002/hc.20620

Reference yield: 96.0%

trimethylsilyl bis(perhydroazepinomethyl)phosphinate → bis(perhydroazepinomethyl)phosphinic acid (244201-57-8)

Guidance literature:

With methanol; In diethyl ether; for 0.25h; Heating;

Refernces

• 1、 Prishchenko,Livantsov,Pol'shchikov,Grigor'ev,Nikolaev,Kustrya. "Phosphorus-substituted derivatives of N-methylhexamethylenimine containing a PCH2N group". . p. 333 - 335. Retrieved 2007/10/03.