[1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride

Base Information

Chemical Name:[1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride
CAS No.:904678-41-7
Molecular Formula:C₁₄H₂₁N₅O*ClH
Molecular Weight:311.815
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride

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Technology Process of [1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride

There total 2 articles about [1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

: 904678-65-5
{3-(3-tert-butyldimethylsilyloxypropyl)-1-[1-(1-tert-butyloxycarbonyl)piperidin-4-yl]imidazolidin-2-ylidene}malononitrile

: 904678-41-7
[1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; for 4h; Product distribution / selectivity;

Reference yield: 92.7%

: 904678-40-6
{1-(1-benzylpiperidin-4-yl)-3-[3-(tert-butyldimethylsilyloxy)propyl]-2-ylidene}malononitrile

: 904678-41-7
[1-(3-Hydroxypropyl)-3-(piperidin-4-yl)imidazolidin-2-ylidene]malononitrile hydrochloride

Guidance literature:: {1-(1-benzylpiperidin-4-yl)-3-[3-(tert-butyldimethylsilyloxy)propyl]-2-ylidene}malononitrile; With carbonochloridic acid 1-chloro-ethyl ester; In 1,2-dichloro-ethane; for 1h; Heating / reflux;

With methanol; for 0.7h; Product distribution / selectivity; Heating / reflux;