Technology Process of 5'-Deoxypyridoxal
There total 6 articles about 5'-Deoxypyridoxal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate; (Mn,Ti)O2 / ethanol / 3 h / 0 - 20 °C / Inert atmosphere
1.2: 4 h / 20 °C / pH 3.5
2.1: hydroxylamine hydrochloride; sodium acetate monohydrate / water
With
sodium tetrahydroborate; sodium acetate monohydrate; (Mn,Ti)O2; hydroxylamine hydrochloride;
In
ethanol; water;
DOI:10.1039/c5ra25779d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate; (Mn,Ti)O2 / ethanol / 3 h / 0 - 20 °C
1.2: 4 h / 20 °C / pH 3.5
2.1: hydroxylamine hydrochloride; sodium acetate monohydrate / water
With
sodium tetrahydroborate; sodium acetate monohydrate; (Mn,Ti)O2; hydroxylamine hydrochloride;
In
ethanol; water;
DOI:10.1039/c5ra25779d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate; (Mn,Ti)O2 / ethanol / 3 h / 0 - 20 °C
1.2: 4 h / 20 °C / pH 3.5
2.1: hydroxylamine hydrochloride; sodium acetate monohydrate / water
With
sodium tetrahydroborate; sodium acetate monohydrate; (Mn,Ti)O2; hydroxylamine hydrochloride;
In
ethanol; water;
DOI:10.1039/c5ra25779d