C₁₅H₁₂N₂O*BrH

Base Information

Chemical Name:C₁₅H₁₂N₂O*BrH
CAS No.:1450606-06-0
Molecular Formula:BrH*C₁₅H₁₂N₂O
Molecular Weight:317.185
Hs Code.:

C<sub>15</sub>H<sub>12</sub>N<sub>2</sub>O*BrH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₂N₂O*BrH

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Technology Process of C₁₅H₁₂N₂O*BrH

There total 2 articles about C₁₅H₁₂N₂O*BrH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7742-73-6
1,3-dichloroisoquinoline

: 1450606-06-0
C₁₅H₁₂N₂O*BrH

Guidance literature:: Multi-step reaction with 5 steps

1: nitric acid; sulfuric acid / water / 2 h / 0 - 5 °C

2: sodium / 16 h / Reflux

3: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene / 48 h / 100 °C

4: palladium 10% on activated carbon; hydrogen / ethanol

5: acetic acid; hydrogen bromide

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; palladium 10% on activated carbon; hydrogen bromide; hydrogen; nitric acid; sodium; acetic acid; In ethanol; water; toluene; 3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmc.2015.06.061