C₃₆H₅₀F₁₀N₂O₂₄

Base Information

Chemical Name:C₃₆H₅₀F₁₀N₂O₂₄
CAS No.:1582775-66-3
Molecular Formula:C₃₆H₅₀F₁₀N₂O₂₄
Molecular Weight:1084.78
Hs Code.:

C<sub>36</sub>H<sub>50</sub>F<sub>10</sub>N<sub>2</sub>O<sub>24</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₅₀F₁₀N₂O₂₄

Chemical Property:

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Technology Process of C₃₆H₅₀F₁₀N₂O₂₄

There total 23 articles about C₃₆H₅₀F₁₀N₂O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1582775-63-0
C₃₀H₄₂F₁₀N₂O₁₈

: 2616-64-0,7305-43-3,50722-58-2,106864-00-0,14520-48-0,30329-32-9,3545-73-1,5918-40-1
uridine diphosphoglucuronic acid

: 1582775-66-3
C₃₆H₅₀F₁₀N₂O₂₄

Guidance literature:: With Pasteurella multocida heparan synthase; manganese(ll) chloride; In aq. buffer; at 20 ℃; pH=7.2; Enzymatic reaction;
DOI:10.1021/ol500738g

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 1582775-66-3
C₃₆H₅₀F₁₀N₂O₂₄

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium azide; trifluoromethylsulfonic anhydride; copper(II) sulfate; triethylamine / acetonitrile; water / 0 - 20 °C

2.1: Amberlite resin (H⁺) / 72 h / Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4.1: pyridine; dmap / 0 - 20 °C / Inert atmosphere

5.1: sodium methylate / methanol / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 20 °C / Inert atmosphere

7.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

8.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

8.2: 2 h / 0 - 20 °C / Inert atmosphere

9.1: pyridine; hydrogen fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

10.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C

11.1: dihydrogen peroxide; lithium hydroxide / water; tetrahydrofuran / -5 - 20 °C

11.2: 0 - 20 °C

12.1: palladium 10% on activated carbon; hydrogen / methanol / 72 h / 20 °C

13.1: triethylamine / water; tetrahydrofuran / 20 °C

14.1: Escherichia coli glycosyltransferase; manganese(ll) chloride / aq. buffer / 20 °C / pH 7.2 / Enzymatic reaction

15.1: manganese(ll) chloride; Pasteurella multocida heparan synthase / aq. buffer / 20 °C / pH 7.2 / Enzymatic reaction

With pyridine; triethylsilane; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium azide; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; boron trifluoride diethyl etherate; Escherichia coli glycosyltransferase; Pasteurella multocida heparan synthase; hydrogen fluoride; hydrogen; dihydrogen peroxide; sodium methylate; sodium hydride; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; manganese(ll) chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol500738g

Reference yield:

: 2-azido-2-deoxy-D-glucose

: 1582775-66-3
C₃₆H₅₀F₁₀N₂O₂₄

Guidance literature:: Multi-step reaction with 14 steps

1.1: Amberlite resin (H⁺) / 72 h / Reflux; Inert atmosphere

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: pyridine; dmap / 0 - 20 °C / Inert atmosphere

4.1: sodium methylate / methanol / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

7.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

7.2: 2 h / 0 - 20 °C / Inert atmosphere

8.1: pyridine; hydrogen fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

9.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C

10.1: dihydrogen peroxide; lithium hydroxide / water; tetrahydrofuran / -5 - 20 °C

10.2: 0 - 20 °C

11.1: palladium 10% on activated carbon; hydrogen / methanol / 72 h / 20 °C

12.1: triethylamine / water; tetrahydrofuran / 20 °C

13.1: Escherichia coli glycosyltransferase; manganese(ll) chloride / aq. buffer / 20 °C / pH 7.2 / Enzymatic reaction

14.1: manganese(ll) chloride; Pasteurella multocida heparan synthase / aq. buffer / 20 °C / pH 7.2 / Enzymatic reaction

With pyridine; triethylsilane; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; boron trifluoride diethyl etherate; Escherichia coli glycosyltransferase; Pasteurella multocida heparan synthase; hydrogen fluoride; hydrogen; dihydrogen peroxide; sodium methylate; sodium hydride; toluene-4-sulfonic acid; triethylamine; manganese(ll) chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol500738g