(S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)

Base Information

Chemical Name:(S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)
CAS No.:66007-19-0
Molecular Formula:C₁₇H₃₂O
Molecular Weight:252.44
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)

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Technology Process of (S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)

There total 27 articles about (S,E)-(+)-14-methyl-8-hexadecenal (trogodermal) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 66007-18-9
(S,E)-(+)-14-methyl-8-hexadecen-1-ol

: 66007-19-0,60609-52-1
(S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In chlorosulfonic acid; dimethyl sulfoxide; at 20 ℃; for 2h;
DOI:10.1055/s-0033-1338432

Reference yield:

: (S)-14-methyl-8-hexadecen-1-ol

: 66007-17-8,60609-52-1
(S)-14-Methyl-(Z)-8-hexadecenal

: 66007-19-0,60609-52-1
(S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)

Guidance literature:: With sodium acetate; silica gel; pyridinium chlorochromate; In dichloromethane; at 0 - 5 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2009.02.064

Reference yield:

: 2-[(S)-14-methylhexadec-8-ynyloxy]tetrahydro-2H-pyran

: 66007-19-0,60609-52-1
(S,E)-(+)-14-methyl-8-hexadecenal (trogodermal)

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / 1 h / 0 - 20 °C / Inert atmosphere

2: sodium; ammonia / tetrahydrofuran / 12 h / -33 °C / Inert atmosphere

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; chlorosulfonic acid / 2 h / 20 °C

With ammonia; sodium; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; chlorosulfonic acid; dimethyl sulfoxide;
DOI:10.1055/s-0033-1338432