(SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan

Base Information

• Chemical Name: (SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan
• CAS No.: 140458-44-2
• Molecular Formula: C₂₆H₃₃NO₂Si
• Molecular Weight: 419.639

Synonyms:

Chemical Property of (SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan

Chemical Property:

Purity/Quality:

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Technology Process of (SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan

There total 3 articles about (SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

(R)-1-(1-naphthyl)ethyl isocyanate (42340-98-7) + rac-(SiR,CR/SiS,CS)-t-butyl(1-hydroxyethyl)methylphenylsilan (614719-66-3) → (SiR,CR,C'R)-t-butylmethyl<1-ethyl>phenylsilan (140458-44-2,140631-61-4) + (SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan (140458-44-2,140631-61-4)

Guidance literature:

at 80 ℃; for 1h;

DOI:10.1016/0022-328X(92)80002-F

Reference yield: 38.0%

(R)-1-(1-naphthyl)ethyl isocyanate (42340-98-7) + rac-(SiR,CR/SiS,CS)-t-butyl(1-hydroxyethyl)methylphenylsilan (614719-66-3) → (SiR,CR,C'R)-t-butylmethyl<1-ethyl>phenylsilan (140458-44-2,140631-61-4) + (SiS,CS,C'R)-t-butylmethyl<1-ethyl>phenylsilan (140458-44-2,140631-61-4)

Guidance literature:

at 80 ℃; for 1h;

DOI:10.1016/0022-328X(92)80002-F

Reference yield:

(R)-1-(1-naphthyl)ethyl isocyanate (42340-98-7) + (SiR,CR)-t-butyl(1-hydroxyethyl)methylphenylsilan (133907-51-4) → (SiR,CR,C'R)-t-butylmethyl<1-ethyl>phenylsilan (140458-44-2,140631-61-4)

Guidance literature:

at 80 ℃; for 1h;

DOI:10.1016/0022-328X(92)80002-F

upstream raw materials:

(R)-1-(1-naphthyl)ethyl isocyanate

rac-(SiR,CR/SiS,CS)-t-butyl(1-hydroxyethyl)methylphenylsilan

(SiR,CR)-t-butyl(1-hydroxyethyl)methylphenylsilan

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