C₃₃H₃₉N₃O₃

Base Information

Chemical Name:C₃₃H₃₉N₃O₃
CAS No.:1367362-99-9
Molecular Formula:C₃₃H₃₉N₃O₃
Molecular Weight:525.691
Hs Code.:

C<sub>33</sub>H<sub>39</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₉N₃O₃

Chemical Property:

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Technology Process of C₃₃H₃₉N₃O₃

There total 16 articles about C₃₃H₃₉N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23521-81-5,17159-82-9
(1,4-dioxaspiro[4.5]dec-8-yl)methanol

: 1367362-99-9
C₃₃H₃₉N₃O₃

: 1367362-98-8
C₃₃H₃₉N₃O₃

Guidance literature:: Multi-step reaction with 11 steps

1: triethylamine / dichloromethane

2: lithium diisopropyl amide

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water

4: diphenyl phosphoryl azide; triethylamine / toluene

5: palladium on activated charcoal; hydrogen / methanol

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

7: palladium on activated charcoal; hydrogen / ethanol

8: triethylamine / dichloromethane

9: sodium hydride / N,N-dimethyl-formamide

10: trifluoroacetic acid / water

11: L-Selectride / tetrahydrofuran

With diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; L-Selectride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: Evan's asymmetric alkylation / 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014

Reference yield:

: 881210-48-6
C₂₄H₃₃NO₅

: 1367362-99-9
C₃₃H₃₉N₃O₃

: 1367362-98-8
C₃₃H₃₉N₃O₃

Guidance literature:: Multi-step reaction with 9 steps

1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water

2: diphenyl phosphoryl azide; triethylamine / toluene

3: palladium on activated charcoal; hydrogen / methanol

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

5: palladium on activated charcoal; hydrogen / ethanol

6: triethylamine / dichloromethane

7: sodium hydride / N,N-dimethyl-formamide

8: trifluoroacetic acid / water

9: L-Selectride / tetrahydrofuran

With diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; L-Selectride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014

Reference yield:

: 1367362-90-0
C₂₆H₃₂N₂O₆

: 1367362-99-9
C₃₃H₃₉N₃O₃

: 1367362-98-8
C₃₃H₃₉N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1: palladium on activated charcoal; hydrogen / ethanol

2: triethylamine / dichloromethane

3: sodium hydride / N,N-dimethyl-formamide

4: trifluoroacetic acid / water

5: L-Selectride / tetrahydrofuran

With palladium on activated charcoal; hydrogen; L-Selectride; sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.014