Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

Base Information

Chemical Name:Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)
CAS No.:186379-78-2
Molecular Formula:C₁₉H₁₄Mo₂O₆
Molecular Weight:530.197
Hs Code.:

Synonyms:

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Chemical Property of Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

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Technology Process of Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

There total 1 articles about Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: ((CH₃)2C)((C₆H₅)2Si)(C₅H₄)2

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 186379-78-2
Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

: 627529-04-8
(Me2C)(Ph2Si)[(η5-C5H3)Mo(CO)3]2

Guidance literature:: In xylene; soln. (Me2C)(Ph2Si)(C5H4)2 and Mo(CO)6 in xylene was refluxed for 6.5 h; sovent was removed, residue was chromed. on alumina (petroleum ether/CH2Cl2); elem. anal.;
DOI:10.1021/om034039z

Reference yield: 20.0%

: 186379-78-2
Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

: 603-35-0
triphenylphosphine

: 211798-28-6
Mo2(CO)5(triphenylphosphine)(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

: 211798-36-6
Mo2(CO)4(triphenylphosphine)2(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

Guidance literature:: In benzene; Irradiation (UV/VIS); N2-atmosphere; irradiation of equimolar amts. (medium pressure Hg-lamp, 110 min, IR monitoring); concn., chromy. (SiO2, petroleum ether or heptane, then C6H6, then C6H6/heptane=3:2); elem. anal.;
DOI:10.1016/S0022-328X(98)00396-9

Reference yield:

: 186379-78-2
Mo2(CO)6(μ-η(5),η(5)-C5H4C(CH3)2C5H4)

: 12176-06-6
hydrido(tricarbonyl)(cyclopentadienyl)molybdenum

: 186379-82-8
[Mo(CO)3H]2(η,η(5)-C5H4C(Me)2C5H4)

Guidance literature:: With Na/K alloy; KHSO₄; In tetrahydrofuran; N2-atmosphere; stirring Mo-complex with excess Na/K alloy (room temp., 4h), filtration (Celite), addn. of excess KHSO4, stirring for 3 h; filtration, solvent removal, drying (vac., overnight);
DOI:10.1016/S0022-328X(96)06277-8