Co3(μ3-CCO2H)(μ-dppm)(CO)7

Base Information

Chemical Name:Co3(μ3-CCO2H)(μ-dppm)(CO)7
CAS No.:794526-46-8
Molecular Formula:C₃₄H₂₃Co₃O₉P₂
Molecular Weight:814.478
Hs Code.:

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Chemical Property of Co3(μ3-CCO2H)(μ-dppm)(CO)7

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Technology Process of Co3(μ3-CCO2H)(μ-dppm)(CO)7

There total 1 articles about Co3(μ3-CCO2H)(μ-dppm)(CO)7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 794526-42-4,558482-40-9
[Co3(μ3-CBr)(μ-bis(diphenylphosphino)methane)(CO)7]

: C₂(CCAuPPh₃)4

: ((OC)7(μ-dppm)Co3-μ-3-CCC)2C=C(CCH)(CC-μ-3-CCo3(μ-dppm)(CO)7)

: 794526-46-8
Co3(μ3-CCO2H)(μ-dppm)(CO)7

: ((OC)7(μ-dppm)Co3-μ-3-CCC)(HCC)C=C(CCAu(PPh3))(CC-μ-3-CCo3(μ-dppm)(CO)7)

: ((OC)7(μ-dppm)Co3-μ-3-CCC)2C=C(CCAu(PPh3))(CC-μ-3-CCo3(μ-dppm)(CO)7)

Guidance literature:: With Pd(PPh₃)4; CuI; In tetrahydrofuran; under N2; Pd(PPh3)4 and CuI added to mixt. of Au complex and Co complex (molar ratio 0.4:0.4:1:4) in THF; stirred at room temp. overnight; filtered; filtrate evapd.; taken up in CH2Cl2; sepd. by preparative thinlayer chromy. (silica gel, acetone-hexane 3:7); magenta band collected, crystd. from CH2Cl2-MeCN; second blue band collected, crystd. from CHCl 3-MeOH; elem. anal.;
DOI:10.1016/j.jorganchem.2006.06.037