chloropentakis(2,6-dimethylphenyl isocyanide)iron(II) tetrachloroferrate(III)

Base Information

• Chemical Name: chloropentakis(2,6-dimethylphenyl isocyanide)iron(II) tetrachloroferrate(III)
• CAS No.: 109168-59-4
• Molecular Formula: C₄₅H₄₅ClFeN₅*Cl₄Fe
• Molecular Weight: 944.845
• Mol file: 109168-59-4.mol

Synonyms:

Chemical Property of chloropentakis(2,6-dimethylphenyl isocyanide)iron(II) tetrachloroferrate(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chloropentakis(2,6-dimethylphenyl isocyanide)iron(II) tetrachloroferrate(III)

There total 1 articles about chloropentakis(2,6-dimethylphenyl isocyanide)iron(II) tetrachloroferrate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) + iron(II) chloride → trans-dichlorotetrakis(2,6-dimethylphenyl isocyanide)iron(II) (109168-57-2,1245576-25-3) + chloropentakis(2,6-dimethylphenyl isocyanide)iron(II) tetrachloroferrate(III) (109168-59-4)

Guidance literature:

In methanol; (N2); xyly isocyanide added dropwise at 0°C; stirred; warmed to room temp.; stirred at room temp. for several days; pptd.; collected; washed (n-hexane); dried in vacuo; decanted soln.; pptd.; collected; recrystd. (hot methanol); elem. anal.;

DOI:10.1016/0022-328X(86)80361-8

upstream raw materials:

2,6-dimethylphenyl isonitrile