Technology Process of C30H29NO9
There total 8 articles about C30H29NO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 12 h
2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 12 h
3: triethylamine / tetrahydrofuran / 12 h
4: triethylamine / methanol / 12 h / 20 °C
5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C
6: sodium methylate / methanol
With
di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; sodium methylate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; pyridine; methanol;
5: Mitsunobu reaction;
DOI:10.1021/jm200148p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / tetrahydrofuran
2: triethylamine / tetrahydrofuran / 12 h
3: triethylamine / methanol / 12 h / 20 °C
4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C
5: sodium methylate / methanol
With
thionyl chloride; di-isopropyl azodicarboxylate; sodium methylate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol;
4: Mitsunobu reaction;
DOI:10.1021/jm200148p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 12 h
2: triethylamine / methanol / 12 h / 20 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C
4: sodium methylate / methanol
With
di-isopropyl azodicarboxylate; sodium methylate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol;
3: Mitsunobu reaction;
DOI:10.1021/jm200148p
