3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone

Base Information

Chemical Name:3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone
CAS No.:119146-32-6
Molecular Formula:C₂₉H₂₈OS₃
Molecular Weight:488.739
Hs Code.:

3-<1-<bis(phenylthio)methylidene>-5-(phenylthio)cyclopentan-2-yl>cyclopentanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone

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Technology Process of 3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone

There total 4 articles about 3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1212-08-4
S-Phenyl benzenethiosulfonate

: 119146-32-6,119239-75-7,119239-76-8,119239-77-9
3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min

2: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min, 2.) 0.5 h

With n-butyllithium;
DOI:10.1021/jo00267a013

Reference yield:

: 3400-45-1
cyclopentanecarboxylic acid

: 119146-32-6,119239-75-7,119239-76-8,119239-77-9
3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Me₃Al / 1.) toluene, xylene, reflux, 19 h, 2. reflux

2: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min

3: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min, 2.) 0.5 h

With n-butyllithium; trimethylaluminum;
DOI:10.1021/jo00267a013

Reference yield:

: 119145-99-2
1-cyclopentane

: 119146-32-6,119239-75-7,119239-76-8,119239-77-9
3-<1--5-(phenylthio)cyclopentan-2-yl>cyclopentanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min

2: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min, 2.) 0.5 h

With n-butyllithium;
DOI:10.1021/jo00267a013