3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene

Base Information Edit

Chemical Name:3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene
CAS No.:183230-89-9
Molecular Formula:C₂₄H₂₀NOPS
Molecular Weight:401.469
Hs Code.:
Mol file:183230-89-9.mol

Synonyms:

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Chemical Property of 3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene Edit

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Technology Process of 3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene

There total 3 articles about 3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 719-80-2
Ethyl diphenylphosphinite

: 183230-86-6
N-benzylthiophene-2-carbimidoyl chloride

: 183230-89-9
3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene

Guidance literature:: at 135 - 140 ℃; for 1.5h;

Reference yield:

: 10354-43-5
thiophene-2-carboxylic acid benzylamide

: 183230-89-9
3-(diphenylphosphinoyl)-1-phenyl-3-(2-thienyl)-2-azapropene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / SOCl₂ / 75 - 80 °C

2: 35 percent / 1.5 h / 135 - 140 °C

With thionyl chloride;