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Technology Process of RhCl3((C6H5)2PCH2CH2SC6H5)2

RhCl3((C6H5)2PCH2CH2SC6H5)2

Base Information
  • Chemical Name:RhCl3((C6H5)2PCH2CH2SC6H5)2
  • CAS No.:90502-23-1
  • Molecular Formula:C40H38Cl3P2RhS2
  • Molecular Weight:854.086
  • Hs Code.:
RhCl<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>SC<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of RhCl3((C6H5)2PCH2CH2SC6H5)2
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Technology Process of RhCl3((C6H5)2PCH2CH2SC6H5)2

There total 1 articles about RhCl3((C6H5)2PCH2CH2SC6H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

trans-[RhCl(CO)(Ph<sub>2</sub>PCH<sub>2</sub>CH<sub>2</sub>SPh)2]
77397-41-2

trans-[RhCl(CO)(Ph2PCH2CH2SPh)2]

mercury dichloride

mercury dichloride

Rh<sup>(1+)</sup>*Hg<sup>(2+)</sup>*3Cl<sup>(1-)</sup>*2(C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>SC<sub>6</sub>H<sub>5</sub>=RhCl<sub>2</sub>(HgCl)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>SC<sub>6</sub>H<sub>5</sub>)2

Rh(1+)*Hg(2+)*3Cl(1-)*2(C6H5)2PCH2CH2SC6H5=RhCl2(HgCl)((C6H5)2PCH2CH2SC6H5)2

RhCl<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>SC<sub>6</sub>H<sub>5</sub>)2
90502-23-1

RhCl3((C6H5)2PCH2CH2SC6H5)2

Guidance literature:
In acetone; byproducts: Hg; HgCl2 adding under N2 to a suspn. of Rh complex in acetone, stirring for 1 h, yellow ppt. filtering off, mother liquor evapg. to dryness under N2, dissolving in CH2Cl2, diluting with ether, yellow ppt. sepg.; identified by elem. anal., IR and NMR spectra;
upstream raw materials:

trans-[RhCl(CO)(Ph2PCH2CH2SPh)2]

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