Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)⁽¹⁺⁾*PF₆^(1-)=[Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)]PF₆

Base Information

• Chemical Name: Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)⁽¹⁺⁾*PF₆^(1-)=[Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)]PF₆
• CAS No.: 80506-69-0
• Molecular Formula: C₄₅H₄₃NiP₂*F₆P
• Molecular Weight: 849.438
• Mol file: 80506-69-0.mol

Synonyms:

Chemical Property of Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)⁽¹⁺⁾*PF₆^(1-)=[Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)⁽¹⁺⁾*PF₆^(1-)=[Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)]PF₆

There total 1 articles about Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)⁽¹⁺⁾*PF₆^(1-)=[Ni(CHCH₃P(C₆H₅)3)2(C₅H₅)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

ammonium hexafluorophosphate + nickelocene (1271-28-9) + ethylenetriphenylphosphorane (1754-88-7) → Ni(CHCH3P(C6H5)3)2(C5H5)(1+)*PF6(1-)=[Ni(CHCH3P(C6H5)3)2(C5H5)]PF6 (80506-69-0)

Guidance literature:

In diethyl ether; acetone; phosphorane in Et2O was added to the nickelocene soln. in Et2O and stirred for 1 h at room temp. under N2,the mixt. was allowed to stay overnight, then the solvent was decanted off and NH4PF6 in acetone was added; filtration, pptn. by addn. of water to the filtrate, ppt. recrystd. from acetone/water;

DOI:10.1016/S0022-328X(00)90111-6

upstream raw materials:

nickelocene

ethylenetriphenylphosphorane