[(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂]^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=[(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂][((C₆H₅)3P)2N]

Base Information

• Chemical Name: [(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂]^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=[(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂][((C₆H₅)3P)2N]
• CAS No.: 309948-73-0
• Molecular Formula: C₁₈H₃₁Cl₂O₆P₂Sn*C₃₆H₃₀NP₂
• Molecular Weight: 1133.59
• Mol file: 309948-73-0.mol

Synonyms:

Chemical Property of [(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂]^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=[(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂][((C₆H₅)3P)2N]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂]^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=[(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂][((C₆H₅)3P)2N]

There total 2 articles about [(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂]^(1-)*((C₆H₅)3P)2N⁽¹⁺⁾=[(P(O)(OC₂H₅)2)2((CH₃)3C)C₆H₂SnCl₂][((C₆H₅)3P)2N] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(2,6-Bis(diethoxyphosphonyl)-4-tert-butyl)phenyl]lithium → [(P(O)(OC2H5)2)2((CH3)3C)C6H2SnCl2](1-)*((C6H5)3P)2N(1+)=[(P(O)(OC2H5)2)2((CH3)3C)C6H2SnCl2][((C6H5)3P)2N] (309948-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: ⁽²⁾H₈-toluene

In tetrahydrofuran; ⁽²⁾H₈-toluene;

DOI:10.1021/om000452k

Reference yield:

([2,6-Bis(diethoxyphosphonyl)-4-tert-butyl]phenyl)tin(II) Chloride (226941-32-8) + bis(triphenylphosphine)iminium chloride (21050-13-5) → [(P(O)(OC2H5)2)2((CH3)3C)C6H2SnCl2](1-)*((C6H5)3P)2N(1+)=[(P(O)(OC2H5)2)2((CH3)3C)C6H2SnCl2][((C6H5)3P)2N] (309948-73-0)

Guidance literature:

In ⁽²⁾H₈-toluene; (Ph3P)2NCl added to soln. of tin compd. in toluene-d8 at room temp. in 1:2 and 1:1 molar ratio; not isolated; NMR monitoring;

DOI:10.1021/om000452k

upstream raw materials:

([2,6-Bis(diethoxyphosphonyl)-4-tert-butyl]phenyl)tin(II) Chloride

bis(triphenylphosphine)iminium chloride