1-[(N-methyl-N-4-bromophenyl)amino]ethylferrocene

Base Information

• Chemical Name: 1-[(N-methyl-N-4-bromophenyl)amino]ethylferrocene
• CAS No.: 616890-93-8
• Molecular Formula: C₁₉H₂₀BrFeN
• Molecular Weight: 398.125
• Mol file: 616890-93-8.mol

Synonyms:

Chemical Property of 1-[(N-methyl-N-4-bromophenyl)amino]ethylferrocene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1-[(N-methyl-N-4-bromophenyl)amino]ethylferrocene

There total 1 articles about 1-[(N-methyl-N-4-bromophenyl)amino]ethylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

sodium tetrahydroborate (16940-66-2) + (C5H5)Fe(C5H4)C(CH3)N(CH3)C6H4Br(1+)*I(1-)=[(C5H5)Fe(C5H4)C(CH3)N(CH3)C6H4Br]I → 1-[(N-methyl-N-4-bromophenyl)amino]ethylferrocene (616890-93-8)

Guidance literature:

In ethanol; mixt. was stirred at room temp. until the bubble ceased; water was added, ppt. was filtered off, water fraction was extd. with chloroform, combined with organic phase, solvent was removed, ppt. was recrystd. from chloroform/EtOH; elem. anal.;

DOI:10.1016/S0022-328X(03)00552-7

upstream raw materials:

sodium tetrahydroborate