{⁽⁹⁹⁾TcN((N(CH₃)2)2CNH)2(SC₆H(CH₃)4)2}

Base Information

Chemical Name:{⁽⁹⁹⁾TcN((N(CH₃)2)2CNH)2(SC₆H(CH₃)4)2}
CAS No.:126217-83-2
Molecular Formula:C₃₀H₅₂N₇S₂Tc
Molecular Weight:673.922
Hs Code.:

{<sup>(99)</sup>TcN((N(CH<sub>3</sub>)2)2CNH)2(SC<sub>6</sub>H(CH<sub>3</sub>)4)2}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {⁽⁹⁹⁾TcN((N(CH₃)2)2CNH)2(SC₆H(CH₃)4)2}

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Technology Process of {⁽⁹⁹⁾TcN((N(CH₃)2)2CNH)2(SC₆H(CH₃)4)2}

There total 1 articles about {⁽⁹⁹⁾TcN((N(CH₃)2)2CNH)2(SC₆H(CH₃)4)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 95012-25-2
[As(C₆H₅)4][(99g)Tc(N)Cl₄]

: 14786-84-6
2,3,5,6-tetramethylthiophenol

: 80-70-6
N,N,N',N'-tetramethylguanidine

: 126217-83-2
{⁽⁹⁹⁾TcN((N(CH₃)2)2CNH)2(SC₆H(CH₃)4)2}

Guidance literature:: In dichloromethane; Over a period of 10 min TMG is added dropwise under N2 to a stirred soln. of the Tc-compd. and Htmbt in CH2Cl2.; After the color of the mixt. changes from orange to brown and back to orange, an equal volume of hexanes is added and the solvent is evaporated slowly. The crystals are collected, washed with hexanes and dried in vacuo.;