tris[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)cobalt hexafluorophosphate

Base Information

• Chemical Name: tris[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)cobalt hexafluorophosphate
• CAS No.: 97385-59-6
• Molecular Formula: C₄₅H₄₅CoN₃O₃P₂*F₆P
• Molecular Weight: 941.775
• Mol file: 97385-59-6.mol

Synonyms:

Chemical Property of tris[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)cobalt hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tris[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)cobalt hexafluorophosphate

There total 1 articles about tris[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)cobalt hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

ammonium hexafluorophosphate + bis(triphenylphosphine)dichlorocobalt(II) (14126-40-0,22327-14-6) + (2-Hydroxyethyl)isocyanid (32835-59-9) → tris[(2-hydroxyethyl)isocyanide]bis(triphenylphosphane)cobalt hexafluorophosphate (97385-59-6)

Guidance literature:

In methanol; ethanol; dropwise addn. of the isocyanide in ethanol to a suspn. of CoCl2(PPh3)2in ethanol under N2 (room temp.), stirring (30 min), cooling (0°C), addn. of a soln. of NH4PF6 in methanol, pptn.; filtration, washing (CH2Cl2, 5 times), recrystn. (acetone/water); elem.anal.;

upstream raw materials:

bis(triphenylphosphine)dichlorocobalt(II)

(2-Hydroxyethyl)isocyanid