(1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC^5',5't'H,6'r'C²)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2t,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester

Base Information

• Chemical Name: (1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC^5',5't'H,6'r'C²)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2t,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester
• CAS No.: 67814-40-8
• Molecular Formula: C₃₂H₂₈Cl₃NO₅S
• Molecular Weight: 645.003

Synonyms:

Chemical Property of (1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC^5',5't'H,6'r'C²)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2t,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester

Chemical Property:

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Safty Information:

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Useful:

Technology Process of (1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC^5',5't'H,6'r'C²)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2t,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester

There total 2 articles about (1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC^5',5't'H,6'r'C²)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2t,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazodiphenylmethane (908093-98-1) → (1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC5',5't'H,6'r'C2)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2c,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester (67760-98-9,67814-40-8)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂

2: Heating

In dichloromethane;

DOI:10.1021/jo00419a031

Reference yield:

diazodiphenylmethane (908093-98-1) → (1S)-3',3'-dimethyl-7'-oxo-3,3-diphenyl-(1rC5',5't'H,6'r'C2)-spiro[cyclopropane-1,6'-(4-thia-1-aza-bicyclo[3.2.0]heptane)]-2t,2't'-dicarboxylic acid 2-benzyl ester 2'-(2,2,2-trichloro-ethyl) ester (67760-98-9,67814-40-8)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂

2: Heating

In dichloromethane;

DOI:10.1021/jo00419a031

upstream raw materials:

diazodiphenylmethane

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