((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])

Base Information

Chemical Name:((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])
CAS No.:287393-76-4
Molecular Formula:C₃₄H₂₃N₂O₈Os₃P
Molecular Weight:1189.14
Hs Code.:

Synonyms:

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Chemical Property of ((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])

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Technology Process of ((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])

There total 3 articles about ((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)]) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 287393-74-2
(Os3(CO)10[η2-Ph2(o-C6H4)CH=N(CH2)2(o-C5H4N)])

: 287393-77-5
((μ-H)Os3(CO)8[μ-η4-Ph2(o-C6H4)C=N(CH2)2(o-C5H4N)])

: 287393-75-3
(Os3(CO)9[μ-η3-Ph2(o-C6H4)CH=N(CH2)2(o-C5H4N)])

: 287393-76-4
((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])

Guidance literature:: In toluene; Schlenk techniques; soln. of (Os3(CO)10(η2-Ph2(o-C6H4)CH=N(CH2)2(o-C5H4N))) in toluene under N2 was heated to reflux for 2 h; soln. was cooled to room temp., ppt. was filtered off and recrystd. from CH2Cl2/n-hexane, filtrate was subjected to TLC (CH2Cl2/n-hexane); elem. anal.;
DOI:10.1039/a910260o

Reference yield: 17.0%

: 15696-40-9
dodecacarbonyl triosmium

: 163727-46-6
N-[2-(diphenylphosphanyl)benzylidene][2-(2-pyridyl)ethyl]amine

: 287393-75-3
(Os3(CO)9[μ-η3-Ph2(o-C6H4)CH=N(CH2)2(o-C5H4N)])

: 287393-76-4
((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])

: 287393-78-6
(Os2(CO)5(μ-PPh2)[μ-η3-Ph2(o-C6H4)C=N(CH2)2(o-C5H4N)])

Guidance literature:: In neat (no solvent); mixt. of (Os3(CO)12) and Ph2P(o-C6H4)CH=N(CH2)2(o-C5H4N) sealed in Pyrex glass tube under vac. was heated at 120°C for 40 min and then at 160°C; mixt. was cooled, residue was dissolved in dichloromethane and applied to TLC (CH2Cl2/n-hexane); elem. anal.;
DOI:10.1039/a910260o

Reference yield:

: 287393-77-5
((μ-H)Os3(CO)8[μ-η4-Ph2(o-C6H4)C=N(CH2)2(o-C5H4N)])

: 287393-76-4
((μ-H)Os3(CO)8[μ3-η4-Ph2(o-C6H4)CH=NCH2CH(o-C5H4N)])

Guidance literature:: In toluene; Schlenk techniques; soln. of ((μ-H)Os3(CO)8(μ-η4-Ph2P(o-C6H4)CH=N(CH2)2(o-C5H4N))) in toluene was heated under reflux under N2 for 5 h;
DOI:10.1039/a910260o