Technology Process of C17H14FNO3
There total 4 articles about C17H14FNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine tris(hydrogen fluoride);
at 120 ℃;
optical yield given as %de;
Inert atmosphere;
DOI:10.1002/chem.201003320
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,4-diaza-bicyclo[2.2.2]octane; trifluoromethylsulfonic anhydride / dichloromethane / -78 - 20 °C / Inert atmosphere
2: triethylamine tris(hydrogen fluoride) / 120 °C / Inert atmosphere
With
1,4-diaza-bicyclo[2.2.2]octane; trifluoromethylsulfonic anhydride; triethylamine tris(hydrogen fluoride);
In
dichloromethane;
DOI:10.1002/chem.201003320
- Guidance literature:
-
Multi-step reaction with 4 steps
1: osmium(VIII) oxide; potassium hexacyanoferrate(III); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether / water; tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere
2: phthalimide / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
3: 1,4-diaza-bicyclo[2.2.2]octane; trifluoromethylsulfonic anhydride / dichloromethane / -78 - 20 °C / Inert atmosphere
4: triethylamine tris(hydrogen fluoride) / 120 °C / Inert atmosphere
With
1,4-diaza-bicyclo[2.2.2]octane; osmium(VIII) oxide; phthalimide; methanesulfonamide; trifluoromethylsulfonic anhydride; potassium hexacyanoferrate(III); sodium hydrogencarbonate; potassium carbonate; triethylamine tris(hydrogen fluoride); hydroquinidein 1,4-phthalazinediyl diether;
In
dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201003320
