C₅₆H₆₂O₁₂Si

Base Information

Chemical Name:C₅₆H₆₂O₁₂Si
CAS No.:1374984-58-3
Molecular Formula:C₅₆H₆₂O₁₂Si
Molecular Weight:955.187
Hs Code.:

C<sub>56</sub>H<sub>62</sub>O<sub>12</sub>Si

Synonyms:

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Chemical Property of C₅₆H₆₂O₁₂Si

Chemical Property:

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Technology Process of C₅₆H₆₂O₁₂Si

There total 9 articles about C₅₆H₆₂O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361049-60-6
methyl (3R,5R)-5-(tert-butyldimethylsilyloxy)-3-hydroxy-6-heptenoate

: 1374984-59-4
C₅₆H₆₂O₁₂Si

: 1374984-58-3
C₅₆H₆₂O₁₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 19 h / -78 - 20 °C

1.3: 21 h / -78 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

2.2: 21 h / 20 °C

3.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

4.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

4.2: 0.5 h / 0 °C

5.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

6.1: acetone; acetonitrile / 2 h / Irradiation

6.2: 16 h / 20 °C / 760.05 Torr

7.1: t-butyldimethylsiyl triflate / dichloromethane / 14 h / 0 °C

With 4-methyl-morpholine; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; sodium hydride; triethylamine; methyl chloroformate; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-61-7
C₂₂H₃₀O₆Si

: 1374984-59-4
C₅₆H₆₂O₁₂Si

: 1374984-58-3
C₅₆H₆₂O₁₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

1.2: 0.5 h / 0 °C

2.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

3.1: acetone; acetonitrile / 2 h / Irradiation

3.2: 16 h / 20 °C / 760.05 Torr

4.1: t-butyldimethylsiyl triflate / dichloromethane / 14 h / 0 °C

With 4-methyl-morpholine; dmap; t-butyldimethylsiyl triflate; triethylamine; methyl chloroformate; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-71-9
C₁₆H₂₆O₆Si

: 1374984-59-4
C₅₆H₆₂O₁₂Si

: 1374984-58-3
C₅₆H₆₂O₁₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

1.2: 21 h / 20 °C

2.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

3.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

3.2: 0.5 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

5.1: acetone; acetonitrile / 2 h / Irradiation

5.2: 16 h / 20 °C / 760.05 Torr

6.1: t-butyldimethylsiyl triflate / dichloromethane / 14 h / 0 °C

With 4-methyl-morpholine; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; sodium hydride; triethylamine; methyl chloroformate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889