meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

Base Information

Chemical Name:meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene
CAS No.:506409-49-0
Molecular Formula:C₂₈H₄₀SiSn
Molecular Weight:523.421
Hs Code.:

Synonyms:

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Chemical Property of meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

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Technology Process of meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

There total 3 articles about meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 504435-17-0
benzylmethylsilanediyl-bis(3-tert-butylcyclopentadiene)

: 1185-22-4
bis(diethylamino)dimethyltin

: 506409-49-0,504435-18-1
rac-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

: 506409-49-0,504435-18-1
meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

: 504435-18-1,506409-49-0
meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

Guidance literature:: In diethyl ether; byproducts: NH(C2H5)2; under Ar or N2 atm.; to soln. of BnMeSi(3-t-BuC5H3)2 in Et2O soln. of Me2Sn(NEt2)2 in Et2O slowly added; mixt. stirred for 4-5 h; vol. of soln. reduced (vac.); storage at 0°C; ppt. collected by filtration; mixture of isomers in 8:1:1 ratio;
DOI:10.1016/S0022-328X(02)01653-4

Reference yield: 48.0%

: 504435-17-0
benzylmethylsilanediyl-bis(3-tert-butylcyclopentadiene)

: 1185-22-4
bis(diethylamino)dimethyltin

: 506409-49-0,504435-18-1
rac-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

: 506409-49-0,504435-18-1
meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

: 504435-18-1,506409-49-0
meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

Guidance literature:: In diethyl ether; byproducts: NH(C2H5)2; under Ar or N2 atm.; to soln. of BnMeSi(3-t-BuC5H3)2 in Et2O soln. of Me2Sn(NEt2)2 in Et2O slowly added; mixt. stirred for 4-5 h; vol. of soln. reduced (vac.); storage at 0°C; ppt. collected by filtration; mixture of isomers in 8:1:1 ratio;
DOI:10.1016/S0022-328X(02)01653-4

Reference yield: 48.0%

: 504435-17-0
benzylmethylsilanediyl-bis(3-tert-butylcyclopentadiene)

: 1185-22-4
bis(diethylamino)dimethyltin

: 506409-49-0,504435-18-1
rac-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

: 506409-49-0,504435-18-1
meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

: 504435-18-1,506409-49-0
meso-2,6-di-tert-butyl-8s-benzyl-4,4,8-trimethyl-8-sila-4-stanna-tetrahydro-indacene

Guidance literature:: In diethyl ether; byproducts: NH(C2H5)2; under Ar or N2 atm.; to soln. of BnMeSi(3-t-BuC5H3)2 in Et2O soln. of Me2Sn(NEt2)2 in Et2O slowly added; mixt. stirred for 4-5 h; vol. of soln. reduced (vac.); storage at 0°C; ppt. collected by filtration; mixture of isomers in 8:1:1 ratio;
DOI:10.1016/S0022-328X(02)01653-4