[(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride)

Base Information

Chemical Name:[(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride)
CAS No.:1269772-05-5
Molecular Formula:C₃₀H₃₄F₆N₆O₆*Cl*Gd
Molecular Weight:881.33
Hs Code.:

[(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride)

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Chemical Property of [(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride)

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Technology Process of [(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride)

There total 1 articles about [(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1269772-25-9
(7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid

: 10138-52-0
gadolinium(III) chloride

: 1269772-05-5
[(((7-carboxymethyl-4,10-bis[(2-trifluoromethylphenylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid)(-2H))Gd](chloride)

Guidance literature:: With DOWEX 1X₈; In water; dissolving C compd. in water, acidification to pH 6, addn. of GdCl3, heating under reflux for 3 h, cooling, evapn. under reduced pressure, dissolving in H2O, stirring for 2 h with anion exchange resin (DOWEX 1X8 200-400 MESH Cl, pretreated with 1 M HCl); filtration, lyophilization;
DOI:10.1039/c0dt01232g