C₂₇H₃₆F₂O₄SeSi

Base Information

Chemical Name:C₂₇H₃₆F₂O₄SeSi
CAS No.:1410037-62-5
Molecular Formula:C₂₇H₃₆F₂O₄SeSi
Molecular Weight:569.623
Hs Code.:

C<sub>27</sub>H<sub>36</sub>F<sub>2</sub>O<sub>4</sub>SeSi

Synonyms:

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Chemical Property of C₂₇H₃₆F₂O₄SeSi

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Technology Process of C₂₇H₃₆F₂O₄SeSi

There total 8 articles about C₂₇H₃₆F₂O₄SeSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867367-67-7
N-methoxy-N-methyl-2-(phenylselanyl)acetamide

: C₂₇H₃₆F₂O₄SeSi

: 1410037-62-5
C₂₇H₃₆F₂O₄SeSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -80 °C

1.2: 20 h / -55 °C

2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.92 h / -80 °C

3.1: zinc; chloro-trimethyl-silane / tetrahydrofuran / 0.08 h / 60 °C

3.2: 2 h / 0 - 20 °C

4.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 96 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -80 - 20 °C

5.2: 24 h / -80 °C

6.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.25 h / -80 - 20 °C

7.1: acetonitrile / 14 h / 20 °C

With 2,6-dimethylpyridine; n-butyllithium; chloro-trimethyl-silane; diisobutylaluminium hydride; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: |Reformatsky Reaction / 3.2: |Reformatsky Reaction / 7.1: |Wittig Olefination;
DOI:10.1039/c2cc35876j

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: C₂₇H₃₆F₂O₄SeSi

: 1410037-62-5
C₂₇H₃₆F₂O₄SeSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -80 °C

1.2: 20 h / -55 °C

2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.92 h / -80 °C

3.1: zinc; chloro-trimethyl-silane / tetrahydrofuran / 0.08 h / 60 °C

3.2: 2 h / 0 - 20 °C

4.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 96 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -80 - 20 °C

5.2: 24 h / -80 °C

6.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.25 h / -80 - 20 °C

7.1: acetonitrile / 14 h / 20 °C

With 2,6-dimethylpyridine; n-butyllithium; chloro-trimethyl-silane; diisobutylaluminium hydride; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: |Reformatsky Reaction / 3.2: |Reformatsky Reaction / 7.1: |Wittig Olefination;
DOI:10.1039/c2cc35876j

Reference yield:

: 1410037-47-6
C₁₈H₂₁NO₃Se

: C₂₇H₃₆F₂O₄SeSi

: 1410037-62-5
C₂₇H₃₆F₂O₄SeSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.92 h / -80 °C

2.1: zinc; chloro-trimethyl-silane / tetrahydrofuran / 0.08 h / 60 °C

2.2: 2 h / 0 - 20 °C

3.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 96 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -80 - 20 °C

4.2: 24 h / -80 °C

5.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 0.25 h / -80 - 20 °C

6.1: acetonitrile / 14 h / 20 °C

With 2,6-dimethylpyridine; n-butyllithium; chloro-trimethyl-silane; diisobutylaluminium hydride; zinc; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: |Reformatsky Reaction / 2.2: |Reformatsky Reaction / 6.1: |Wittig Olefination;
DOI:10.1039/c2cc35876j