C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂

Base Information

Chemical Name:C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂
CAS No.:1176086-93-3
Molecular Formula:C₁₇H₃₃Cl₂GeN₃Si₂
Molecular Weight:479.136
Hs Code.:

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>NSi(CH<sub>3</sub>)3)2GeCl<sub>2</sub>

Synonyms:

Suppliers and Price of C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂

There total 2 articles about C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 2Li⁽¹⁺⁾*C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2^(2-)=C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2Li₂

: 10038-98-9
germaniumtetrachloride

: 1176086-93-3
C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂

Guidance literature:: In toluene; byproducts: LiBr; (Ar, Schlenk) GeBr4 in toluene was added to a Li-compound in toluene at -78°C with stirring, the soln. was stirred for 24 h at room temp.; ppt. was extd. with toluene, detected by NMR spectra;
DOI:10.1039/b901885a

Reference yield:

: 1176086-95-5
C₆H₅CH₂N(CH₂CH₂NHSi(CH₃)3)2

: 10038-98-9
germaniumtetrachloride

: 1176086-93-3
C₆H₅CH₂N(CH₂CH₂NSi(CH₃)3)2GeCl₂

Guidance literature:: With triethyl amine; In toluene; byproducts: (C2H5)3N*HCl; (Ar, Schlenk) to a stirred soln. of GeCl4 in toluene a toluene-soln. of amine and triethylamine in toluene was added dropwise at -78°C, the stirring mixt. was allowed to warm to room temp. overnight; ppt. was filtered, volatiles were evapd. in vac.; detected by NMR spectra;
DOI:10.1039/b901885a