1-dimethylaminomethyl-2-phenylethynylferrocene

Base Information

• Chemical Name: 1-dimethylaminomethyl-2-phenylethynylferrocene
• CAS No.: 380238-57-3
• Molecular Formula: C₂₁H₂₁FeN
• Molecular Weight: 343.251
• Mol file: 380238-57-3.mol

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Chemical Property of 1-dimethylaminomethyl-2-phenylethynylferrocene

Chemical Property:

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Technology Process of 1-dimethylaminomethyl-2-phenylethynylferrocene

There total 1 articles about 1-dimethylaminomethyl-2-phenylethynylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

σ-chloroplatinum(II){CpFe(η5-C5H3CH2NMe2)}(DMSO) + phenylacetylene (536-74-3) → 1-dimethylaminomethyl-2-phenylethynylferrocene (380238-57-3)

Guidance literature:

With lithium diisopropylamide; In tetrahydrofuran; under N2; lithium diisopropylamide added to soln. of phenylacetylene (molar ratio 3:1) in THF; stirred for 30 min at room temp.; 1 equiv. of Pt-Fe complex in THF added slowly; stirred for 8 h; solvent removed in vac.; dissolved in CH2Cl2; recrystd. from ethyl acetate-hexane; elem. anal.;

DOI:10.1039/b101776o

upstream raw materials:

phenylacetylene