trans-(η5-C5H4Me)Mo(CO)2(PPhEt2)I

Base Information

• Chemical Name: trans-(η5-C5H4Me)Mo(CO)2(PPhEt2)I
• CAS No.: 881896-84-0
• Molecular Formula: C₁₈H₂₂IMoO₂P
• Molecular Weight: 524.19

Synonyms:

Chemical Property of trans-(η5-C5H4Me)Mo(CO)2(PPhEt2)I

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Technology Process of trans-(η5-C5H4Me)Mo(CO)2(PPhEt2)I

There total 1 articles about trans-(η5-C5H4Me)Mo(CO)2(PPhEt2)I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(η(5)-(C5H4Me))Mo(CO)3I + diethyl-phenyl-phosphine (1605-53-4) → trans-(η5-C5H4Me)Mo(CO)2(PPhEt2)I (881896-84-0,881738-75-6) + cis-(η5-C5H4Me)Mo(CO)2(PPhEt2)I

Guidance literature:

With trimethylamine N-oxide dihydrate; In dichloromethane; under dry N2 atm. using Schlenk techniques; Mo complex, 5-10-fold excessof phosphine ligand and trimethylamine N-oxide in CH2Cl2 at room temp.; cis- and trans-isomers sepn. was achieved by dissolving in CH2Cl2 followed by mixing with small amt. of silica gel; solvent removed; sepd. by chromy. on column of silica (toluene/hexane, 1:1) as eluent;

DOI:10.1016/j.jorganchem.2005.10.032

upstream raw materials:

diethyl-phenyl-phosphine

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