1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether

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Chemical Name:1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether
CAS No.:107574-20-9
Molecular Formula:C₂₄H₄₇ClLiN₃OSi₄Ti
Molecular Weight:596.273
Hs Code.:

1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether

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Chemical Property of 1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether

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Technology Process of 1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether

There total 1 articles about 1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: phenyltris(trimethylsilyl-N-lithioamino)silane

: 107574-20-9
1,3-bis(trimethylsilyl)-4-chloro-4-η5-cyclopentadienyl-2-(N-lithiotrimethylsilylamino)-2-phenyl-1,3-diaza-2-sila-4-titana-cyclobutane-diethyl ether

Guidance literature:: In diethyl ether; byproducts: LiCl; CpTiCl3 added at -30°C; stirred for 1 h at 30°C then for 2 h at 0°C; LiCl filtered off; concd.; crystals sepd. at -25°C; recrystd. (petroleum ether/toluene); elem. anal.;
DOI:10.1016/0022-328X(86)80472-7