neodymium (N-benzoyl-N'-orthomethoxyphenyl thiocarbamide) chloridehydrate

Base Information

Chemical Name:neodymium (N-benzoyl-N'-orthomethoxyphenyl thiocarbamide) chloridehydrate
CAS No.:85295-21-2
Molecular Formula:C₁₅H₁₂N₂O₂S*Cl*H₂O*Nd
Molecular Weight:482.047
Hs Code.:

Synonyms:

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Chemical Property of neodymium (N-benzoyl-N'-orthomethoxyphenyl thiocarbamide) chloridehydrate

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Technology Process of neodymium (N-benzoyl-N'-orthomethoxyphenyl thiocarbamide) chloridehydrate

There total 2 articles about neodymium (N-benzoyl-N'-orthomethoxyphenyl thiocarbamide) chloridehydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21258-10-6
N-benzoyl-N'-orthomethoxyphenyl thiocarbamide

: 10024-93-8
neodymium trichloride

: 85295-21-2
neodymium (N-benzoyl-N'-orthomethoxyphenyl thiocarbamide) chloridehydrate

Guidance literature:: With NH₄OH; In ethanol; water; aq. ethanolic soln. of metal chloride and ligand were mixed in 1:1 moleratio, the pH of the stirred soln. was adjusted by dropwise addn. of very dil. NH4OH ethanolic soln. to just below pptn. of hydrated hydroxide or oxide for 2 h, refluxed for 6-8 h; ppt. filtered, dried in vac. over CaCl2, elem.anal.;

Reference yield:

: 21258-10-6
N-benzoyl- N′-(2-methoxyphenyl)thiourea

: 10024-93-8
neodymium trichloride

: 85295-21-2
Nd⁽³⁺⁾*C₁₅H₁₂N₂O₂S^(2-)*Cl^(1-)*H₂O=Nd(C₁₅H₁₂N₂O₂S)Cl*H₂O

Guidance literature:: In ethanol; adding ethanolic ammonia, dropwise, to an ethanolic soln. of chloride and ligand (1:1 mole ratio) until pH was just below that required for pptn. of the rare earth hydroxide, mixt. was then heated at reflux for 6-8 h; prepicitate filtrated, washed with water and ethanol and dried in vac. over CaCl2;