3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol

Base Information

Chemical Name:3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol
CAS No.:16134-20-6
Molecular Formula:C₁₁H₁₅NO₆
Molecular Weight:257.243
Hs Code.:

3.5-Bis-<hydroxymethyl>-4-(2.3-dihydroxypropyl)-nitrobenzol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol

Chemical Property:

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Technology Process of 3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol

There total 2 articles about 3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16134-13-7
1-Hydroxy-3.5-diacetoxymethyl-7-nitro-1H-benzopyran-⁽²⁾

: 16134-20-6
3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol

Guidance literature:: With sodium tetrahydroborate;
DOI:10.1021/jo01269a026

Reference yield:

: Acetic acid 5-acetoxymethyl-3,10-dimethoxy-7,11-dinitro-4,9-dioxa-tricyclo[6.2.2.0^2,7]dodeca-5,11-dien-8-ylmethyl ester

: 16134-20-6
3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol

Guidance literature:: Multi-step reaction with 2 steps

1: AcNH₂ / Heating

2: NaBH₄

With acetamide; sodium tetrahydroborate;
DOI:10.1021/jo01269a026

Reference yield:

: 16134-20-6
3.5-Bis--4-(2.3-dihydroxypropyl)-nitrobenzol

: 16134-23-9
4-(2-Hydroxyethyl)-3,5-bis-(hydroxymethyl)-nitrobenzol

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaIO₄

2: NaBH₄

With sodium tetrahydroborate; sodium periodate;
DOI:10.1021/jo01269a026