Bn-Bac

Base Information

Chemical Name:Bn-Bac
CAS No.:68536-16-3
Molecular Formula:C₁₉H₂₆N₂O₆
Molecular Weight:378.425
Hs Code.:

Synonyms:

Suppliers and Price of Bn-Bac

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Bn-Bac

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Bn-Bac

There total 7 articles about Bn-Bac which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: phenyl 2,4-diazido-3-O-acetyl-2,4,6-trideoxy-1-thio-β-D-glucopyranoside

: 68536-16-3
Bn-Bac

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane; diethyl ether / 1 h / 0 °C / Molecular sieve

2: zinc; acetic acid / tetrahydrofuran / 9 h / 20 °C

3: dmap / tetrahydrofuran / 5 h / 0 - 20 °C

With dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; acetic acid; zinc; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/c9sc05955e

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 68536-16-3
Bn-Bac

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane; diethyl ether / 1 h / 0 °C / Molecular sieve

2: zinc; acetic acid / tetrahydrofuran / 9 h / 20 °C

3: dmap / tetrahydrofuran / 5 h / 0 - 20 °C

With dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; acetic acid; zinc; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/c9sc05955e

Reference yield:

: 1432492-20-0
phenyl 3-O-acetyl-6-deoxy-1-thio-β-D-mannopyranoside

: 68536-16-3
Bn-Bac

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / dichloromethane / 1 h / 0 °C

2: tetrabutylammoniun azide / acetonitrile / 18 h / -30 °C

3: potassium nitrite / N,N-dimethyl-formamide / 5 h / 20 °C

4: pyridine / dichloromethane / 1 h / 0 °C

5: sodium azide / N,N-dimethyl-formamide / 5 h / 20 °C

6: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane; diethyl ether / 1 h / 0 °C / Molecular sieve

7: zinc; acetic acid / tetrahydrofuran / 9 h / 20 °C

8: dmap / tetrahydrofuran / 5 h / 0 - 20 °C

With pyridine; dmap; N-iodo-succinimide; sodium azide; potassium nitrite; trifluorormethanesulfonic acid; tetrabutylammoniun azide; acetic acid; zinc; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c9sc05955e