2,4,4-trimethyl-adipic acid-dianilide

Base Information

• Chemical Name: 2,4,4-trimethyl-adipic acid-dianilide
• CAS No.: 115020-70-7
• Molecular Formula: C₂₁H₂₆N₂O₂
• Molecular Weight: 338.45
• Mol file: 115020-70-7.mol

Synonyms:

Chemical Property of 2,4,4-trimethyl-adipic acid-dianilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,4-trimethyl-adipic acid-dianilide

There total 5 articles about 2,4,4-trimethyl-adipic acid-dianilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-Amino-3,3,5-trimethyl-hexansaeure (21260-87-7) → 2,4,4-trimethyl-adipic acid-dianilide (115020-70-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH, KMnO₄

2: (i) SOCl₂, (ii) /BRN= 605631/

With sodium hydroxide; potassium permanganate;

DOI:10.1021/jo01063a603

Reference yield:

4,4,6-trimethylazepan-2-one (21260-88-8) → 2,4,4-trimethyl-adipic acid-dianilide (115020-70-7)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. HBr

2: aq. NaOH, KMnO₄

3: (i) SOCl₂, (ii) /BRN= 605631/

With sodium hydroxide; potassium permanganate; hydrogen bromide;

DOI:10.1021/jo01063a603

Reference yield:

aniline (62-53-3) → 2,4,4-trimethyl-adipic acid-dianilide (115020-70-7)

Guidance literature:

DOI:10.1021/jo01087a618

upstream raw materials:

2,4,4-trimethyl-adipic acid

aniline

6-Amino-3,3,5-trimethyl-hexansaeure

4,4,6-trimethylazepan-2-one