tetrakis[2-N-bis(2,4-dichlorobenzylidene-κC2-amino-κN)benzenethiolato]tetranickel(II)

Base Information

• Chemical Name: tetrakis[2-N-bis(2,4-dichlorobenzylidene-κC2-amino-κN)benzenethiolato]tetranickel(II)
• CAS No.: 680220-39-7
• Molecular Formula: C₅₂H₂₈Cl₈N₄Ni₄S₄
• Molecular Weight: 1355.47

Synonyms:

Chemical Property of tetrakis[2-N-bis(2,4-dichlorobenzylidene-κC2-amino-κN)benzenethiolato]tetranickel(II)

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Technology Process of tetrakis[2-N-bis(2,4-dichlorobenzylidene-κC2-amino-κN)benzenethiolato]tetranickel(II)

There total 1 articles about tetrakis[2-N-bis(2,4-dichlorobenzylidene-κC2-amino-κN)benzenethiolato]tetranickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

bis[2-(2,4-dichlorophenylmethyleneamino)benzenethiolato]nickel(II) → [bis-2,2'-[1,2-bis(2,4-dichlorophenyl)ethylenedidiimine]benzenethiolato]nickel(II) + tetrakis[2-N-bis(2,4-dichlorobenzylidene-κC2-amino-κN)benzenethiolato]tetranickel(II) (680220-39-7)

Guidance literature:

In toluene; under Ar or N2 atm. using Schlenk techniques; suspn. of Ni complex in toluene refluxed for 1.5 h; cooled to room temp.; ppt. filtered off; filtrate purified by chromy. on silica gel column (CH2Cl2 as eluent); first band collected and dried; recrystd. (CHCl3-Et2O);

DOI:10.1246/bcsj.77.289

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