Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester

Base Information

• Chemical Name: Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester
• CAS No.: 122600-23-1
• Molecular Formula: C₂₈H₄₆N₂O₆P₂S₄
• Molecular Weight: 696.895
• Mol file: 122600-23-1.mol

Synonyms:

Chemical Property of Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester

There total 2 articles about Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.3%

1-(chloroacetyl)-2-(2-chloro-N-phenylacetamido)-1,4,5,6-tetrahydropyridine (122600-31-1) + potassium O,O'-dipropyl dithiophosphate (3287-84-1) → Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester (122600-23-1)

Guidance literature:

In acetonitrile; Ambient temperature;

Reference yield:

2-(phenylamino)-3,4,5,6-tetrahydropyridine (67997-72-2) → Dithiophosphoric acid S-[({1-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl}-phenyl-carbamoyl)-methyl] ester O,O'-dipropyl ester (122600-23-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / -20 - -10 °C

2: 35.3 percent / acetonitrile / Ambient temperature

In acetonitrile;

upstream raw materials:

1-(chloroacetyl)-2-(2-chloro-N-phenylacetamido)-1,4,5,6-tetrahydropyridine

potassium O,O'-dipropyl dithiophosphate

2-(phenylamino)-3,4,5,6-tetrahydropyridine