2-Naphthalenamine, 1-[(1-methyl-1H-benzimidazol-2-yl)azo]-N-phenyl-

Base Information

• Chemical Name: 2-Naphthalenamine, 1-[(1-methyl-1H-benzimidazol-2-yl)azo]-N-phenyl-
• CAS No.: 140836-28-8
• Molecular Formula: C₂₄H₁₉N₅
• Molecular Weight: 377.448
• DSSTox Substance ID: DTXSID20385967
• Mol file: 140836-28-8.mol

Synonyms:140836-28-8;2-Naphthalenamine, 1-[(1-methyl-1H-benzimidazol-2-yl)azo]-N-phenyl-;SCHEMBL22822791;DTXSID20385967;[1-(1-Methyl-1H-benzoimidazol-2-ylazo)-naphthalen-2-yl]-phenyl-amine;STL302818;AKOS000562423;1-[(E)-(1-methyl-1H-benzimidazol-2-yl)diazenyl]-N-phenylnaphthalen-2-amine

Chemical Property of 2-Naphthalenamine, 1-[(1-methyl-1H-benzimidazol-2-yl)azo]-N-phenyl-

Chemical Property:

• PSA: 54.57000
• LogP: 6.95850
• XLogP3: 6.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 377.16404563
• Heavy Atom Count: 29
• Complexity: 560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1C2=CC=CC=C2N=C1N=NC3=C(C=CC4=CC=CC=C43)NC5=CC=CC=C5

Technology Process of 2-Naphthalenamine, 1-[(1-methyl-1H-benzimidazol-2-yl)azo]-N-phenyl-

There total 2 articles about 2-Naphthalenamine, 1-[(1-methyl-1H-benzimidazol-2-yl)azo]-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-Phenyl-2-naphthylamine (135-88-6,84420-28-0) + 1-methylbenzimidazole-2-diazonium phosphate → 2-(2'-N-phenylaminonaphthylazo)-1-methylbenzimidazole (140836-28-8)

Guidance literature:

With acetic acid; for 4h; Ambient temperature;

DOI:10.1007/BF00484360

Reference yield: 77.0%

2-(2-methoxynaphthylazo)-1-methylbenzimidazole (122351-31-9) + aniline (62-53-3) → 2-(2'-N-phenylaminonaphthylazo)-1-methylbenzimidazole (140836-28-8)

Guidance literature:

In chloroform; for 38h; Ambient temperature;

DOI:10.1007/BF00484360

Reference yield:

nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) + 2-(2'-N-phenylaminonaphthylazo)-1-methylbenzimidazole (140836-28-8) → Ni(2-(2'-N-phenylaminonaphthylazo)-1-methylbenzimidazole)2 (95179-79-6)

Guidance literature:

In ethanol; heated gently (ratio metal acetate : ligand = 1:2); elem. anal.;

upstream raw materials:

N-Phenyl-2-naphthylamine

2-(2-methoxynaphthylazo)-1-methylbenzimidazole

aniline

Downstream raw materials:

Ni(2-(2'-N-phenylaminonaphthylazo)-1-methylbenzimidazole)2

Cu(2-(2'-N-phenylaminonaphthylazo)-1-methylbenzimidazole)2

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