Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester

Base Information

• Chemical Name: Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester
• CAS No.: 137407-83-1
• Molecular Formula: C₄₈H₅₇N₇O₁₂
• Molecular Weight: 924.02

Synonyms:

Chemical Property of Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester

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Technology Process of Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester

There total 1 articles about Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + Virginiamycin S1 (668-72-4,23152-29-6,117603-96-0) → Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester (137407-83-1)

Guidance literature:

With dmap; In dichloromethane; for 0.0833333h;

Reference yield: 15.0%

Carbonic acid 2-((3S,6S,12R,15S,16R,19S)-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester tert-butyl ester (137407-83-1) → Virginiamycin S1 (668-72-4,23152-29-6,117603-96-0) + (S)-{[1-((S)-2-{[(S)-1-((R)-2-{(2S,3R)-3-Hydroxy-2-[(3-hydroxy-pyridine-2-carbonyl)-amino]-butyrylamino}-butyryl)-pyrrolidine-2-carbonyl]-methyl-amino}-3-phenyl-propionyl)-4-oxo-piperidine-2-carbonyl]-amino}-phenyl-acetic acid (127106-18-7)

Guidance literature:

With sodium hydroxide; for 3h;

upstream raw materials:

di-tert-butyl dicarbonate

Virginiamycin S₁

Downstream raw materials:

Virginiamycin S₁

(S)-{[1-((S)-2-{[(S)-1-((R)-2-{(2S,3R)-3-Hydroxy-2-[(3-hydroxy-pyridine-2-carbonyl)-amino]-butyrylamino}-butyryl)-pyrrolidine-2-carbonyl]-methyl-amino}-3-phenyl-propionyl)-4-oxo-piperidine-2-carbonyl]-amino}-phenyl-acetic acid

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