C₂₀H₃₀N₂O₃S

Base Information

Chemical Name:C₂₀H₃₀N₂O₃S
CAS No.:1572246-85-5
Molecular Formula:C₂₀H₃₀N₂O₃S
Molecular Weight:378.536
Hs Code.:

C<sub>20</sub>H<sub>30</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₀H₃₀N₂O₃S

Chemical Property:

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Technology Process of C₂₀H₃₀N₂O₃S

There total 13 articles about C₂₀H₃₀N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1572246-44-6
(S)-4-methyl-5-[(p-methylbenzenesulfonyl)amino]-1-pentanol

: 1572246-85-5
C₂₀H₃₀N₂O₃S

: 1572246-88-8
C₂₀H₃₀N₂O₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / dichloromethane / 15 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 17 h / 20 °C

3.1: hydrogenchloride / water / 0.33 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

5.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C

5.2: 3 h / 20 °C

6.1: hydrazine hydrate / ethanol / 2.5 h / Reflux

7.1: triethylamine / dichloromethane / 2.5 h / 20 °C

8.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 14 h / Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; potassium tert-butylate; sodium hydride; Dess-Martin periodane; hydrazine hydrate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo5002627

Reference yield:

: 40630-06-6
methyl 4-formylvalerate

: 1572246-85-5
C₂₀H₃₀N₂O₃S

: 1572246-88-8
C₂₀H₃₀N₂O₃S

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium sulfate / diethyl ether / 5 h / 0 °C

2.1: n-butyllithium; borane-ammonia complex / tetrahydrofuran; hexane / 1 h / 0 - 40 °C

3.1: palladium(II) hydroxide; hydrogen / methanol / 18 h / 68 °C / 7500.75 Torr

4.1: triethylamine / dichloromethane / 15 h / 20 °C

5.1: 1H-imidazole / dichloromethane / 15 h / Reflux

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 17 h / 20 °C

7.1: hydrogenchloride / water / 0.33 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

9.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C

9.2: 3 h / 20 °C

10.1: hydrazine hydrate / ethanol / 2.5 h / Reflux

11.1: triethylamine / dichloromethane / 2.5 h / 20 °C

12.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 14 h / Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; n-butyllithium; borane-ammonia complex; potassium tert-butylate; hydrogen; palladium(II) hydroxide; sodium hydride; Dess-Martin periodane; hydrazine hydrate; sodium sulfate; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo5002627

Reference yield:

: 1572245-70-5
(3R,8S,8aR)-8-methyl-5-oxo-3-phenyl-2,3,6,7,8,8a-hexahydro-5H-oxazolo[3,2-a]pyridine

: 1572246-85-5
C₂₀H₃₀N₂O₃S

: 1572246-88-8
C₂₀H₃₀N₂O₃S

Guidance literature:: Multi-step reaction with 11 steps

1.1: n-butyllithium; borane-ammonia complex / tetrahydrofuran; hexane / 1 h / 0 - 40 °C

2.1: palladium(II) hydroxide; hydrogen / methanol / 18 h / 68 °C / 7500.75 Torr

3.1: triethylamine / dichloromethane / 15 h / 20 °C

4.1: 1H-imidazole / dichloromethane / 15 h / Reflux

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 17 h / 20 °C

6.1: hydrogenchloride / water / 0.33 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

8.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C

8.2: 3 h / 20 °C

9.1: hydrazine hydrate / ethanol / 2.5 h / Reflux

10.1: triethylamine / dichloromethane / 2.5 h / 20 °C

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 14 h / Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; n-butyllithium; borane-ammonia complex; potassium tert-butylate; hydrogen; palladium(II) hydroxide; sodium hydride; Dess-Martin periodane; hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo5002627