ethyl(o-methoxymethylbenzyl)dichlorostannane

Base Information

Chemical Name:ethyl(o-methoxymethylbenzyl)dichlorostannane
CAS No.:76077-39-9
Molecular Formula:C₁₁H₁₆Cl₂OSn
Molecular Weight:353.863
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl(o-methoxymethylbenzyl)dichlorostannane

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Technology Process of ethyl(o-methoxymethylbenzyl)dichlorostannane

There total 1 articles about ethyl(o-methoxymethylbenzyl)dichlorostannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 58110-06-8
1-methylene-4-methoxymethyl-2,5-cyclohexadiene

: 58110-05-7
1-methylene-6-methoxymethyl-2,4-cyclohexadiene

: 1066-57-5
ethyltintrichloride

: 76077-39-9
ethyl(o-methoxymethylbenzyl)dichlorostannane

Guidance literature:: In diethyl ether; byproducts: HCl; to stirred soln. of C2H5SnCl3 added dropwise (20 min) soln. of mixt. of1-methylene-6-methoxymethyl-2,4-cyclohexadiene and 1-methylene-4-methoxymethyl-2,5-cyclohexadiene; stirred for another h.; solvent distd. (40-45°C); residue dissolved in benzene; chromd. (silica gel, benzene); evapd.; crystd.; recrystd.(hexane); elem. anal.;
DOI:10.1007/BF01168279