1-[1,1-dimethyl-2,2-bis(trimethylsilyl)-1-germaethyl]-2-[2,2-dimethyl-3,3-bis(trimethylsilyl)-2-germapropyl]-benzene

Base Information

• Chemical Name: 1-[1,1-dimethyl-2,2-bis(trimethylsilyl)-1-germaethyl]-2-[2,2-dimethyl-3,3-bis(trimethylsilyl)-2-germapropyl]-benzene
• CAS No.: 324582-92-5
• Molecular Formula: C₂₅H₅₆Ge₂Si₄
• Molecular Weight: 614.242
• Mol file: 324582-92-5.mol

Synonyms:

Chemical Property of 1-[1,1-dimethyl-2,2-bis(trimethylsilyl)-1-germaethyl]-2-[2,2-dimethyl-3,3-bis(trimethylsilyl)-2-germapropyl]-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[1,1-dimethyl-2,2-bis(trimethylsilyl)-1-germaethyl]-2-[2,2-dimethyl-3,3-bis(trimethylsilyl)-2-germapropyl]-benzene

There total 1 articles about 1-[1,1-dimethyl-2,2-bis(trimethylsilyl)-1-germaethyl]-2-[2,2-dimethyl-3,3-bis(trimethylsilyl)-2-germapropyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

9,10-dihydro-9,10-(11,11-dimethyl-12,12-bis(trimethylsilyl)-11-germaethano)anthracene (103458-12-4) → (benzyldimethylgermyl)bis(trimethylsilyl)methane (220265-30-5) + 1-[1,1-dimethyl-2,2-bis(trimethylsilyl)-1-germaethyl]-2-[2,2-dimethyl-3,3-bis(trimethylsilyl)-2-germapropyl]-benzene (324582-92-5) + 1,1,3,3-tetramethyl-2,2,4,4-tetrakis(trimethylsilyl)-1,3-digermacyclobutane (54008-65-0)

Guidance literature:

In toluene; Ge-complex in toluene was heated at 130°C for 44 d in sealed NMRtube; volatiles were removed, residue was treated with tBuOMe/MeOH, sepd. by HPLC with MeOH; monitored by NMR;

DOI:10.1139/v00-095

upstream raw materials:

9,10-dihydro-9,10-(11,11-dimethyl-12,12-bis(trimethylsilyl)-11-germaethano)anthracene