Technology Process of C45H38F6INO2S2
There total 7 articles about C45H38F6INO2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride; n-butyllithium; Triisopropyl borate / tetrahydrofuran; water / -78 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water
3: n-butyllithium / tetrahydrofuran / -78 °C
4: Iodine monochloride / dichloromethane
5: copper; potassium carbonate / 1,2-dichloro-benzene
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Triisopropyl borate; Iodine monochloride; copper; sodium carbonate; potassium carbonate;
In
tetrahydrofuran; dichloromethane; water; 1,2-dichloro-benzene;
DOI:10.1021/ja207025x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium / tetrahydrofuran / -78 °C
2: Iodine monochloride / dichloromethane
3: copper; potassium carbonate / 1,2-dichloro-benzene
With
n-butyllithium; Iodine monochloride; copper; potassium carbonate;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-benzene;
DOI:10.1021/ja207025x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Iodine monochloride / dichloromethane
2: copper; potassium carbonate / 1,2-dichloro-benzene
With
Iodine monochloride; copper; potassium carbonate;
In
dichloromethane; 1,2-dichloro-benzene;
DOI:10.1021/ja207025x
