Benzene, [(1-nitrononyl)sulfonyl]-

Base Information

• Chemical Name: Benzene, [(1-nitrononyl)sulfonyl]-
• CAS No.: 140846-11-3
• Molecular Formula: C15H23NO4S
• Molecular Weight: 313.418
• Mol file: 140846-11-3.mol

Synonyms:

Chemical Property of Benzene, [(1-nitrononyl)sulfonyl]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene, [(1-nitrononyl)sulfonyl]-

There total 3 articles about Benzene, [(1-nitrononyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-benzenesulfonyl-1-nitronon-2-ene → 1-nitro-1-(phenylsulfonyl)nonane (140846-11-3)

Guidance literature:

With sodium cyanoborohydride; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1016/j.tet.2019.130883

Reference yield:

phenylsulfonylnitromethane (21272-85-5) → 1-nitro-1-(phenylsulfonyl)nonane (140846-11-3)

Guidance literature:

Multi-step reaction with 2 steps

1: L-proline; ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol / dimethyl sulfoxide / 4 h / 40 °C / Sonication

2: sodium cyanoborohydride / N,N-dimethyl-formamide / 90 °C

With ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol; sodium cyanoborohydride; L-proline; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2019.130883

Reference yield:

Octanal (124-13-0) → 1-nitro-1-(phenylsulfonyl)nonane (140846-11-3)

Guidance literature:

Multi-step reaction with 2 steps

1: L-proline; ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol / dimethyl sulfoxide / 4 h / 40 °C / Sonication

2: sodium cyanoborohydride / N,N-dimethyl-formamide / 90 °C

With ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol; sodium cyanoborohydride; L-proline; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2019.130883

upstream raw materials:

phenylsulfonylnitromethane

Octanal

Downstream raw materials:

nonan-1-al

nonanoic acid

nonanamide

nonanoic acid methyl ester