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Benzene, [(1-nitrononyl)sulfonyl]-

Base Information
  • Chemical Name:Benzene, [(1-nitrononyl)sulfonyl]-
  • CAS No.:140846-11-3
  • Molecular Formula:C15H23NO4S
  • Molecular Weight:313.418
  • Hs Code.:
Benzene, [(1-nitrononyl)sulfonyl]-

Synonyms:

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Chemical Property of Benzene, [(1-nitrononyl)sulfonyl]-
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Technology Process of Benzene, [(1-nitrononyl)sulfonyl]-

There total 3 articles about Benzene, [(1-nitrononyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium cyanoborohydride; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1016/j.tet.2019.130883
Guidance literature:
Multi-step reaction with 2 steps
1: L-proline; ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol / dimethyl sulfoxide / 4 h / 40 °C / Sonication
2: sodium cyanoborohydride / N,N-dimethyl-formamide / 90 °C
With ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol; sodium cyanoborohydride; L-proline; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2019.130883
Guidance literature:
Multi-step reaction with 2 steps
1: L-proline; ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol / dimethyl sulfoxide / 4 h / 40 °C / Sonication
2: sodium cyanoborohydride / N,N-dimethyl-formamide / 90 °C
With ester of 3,5-di-tert-butyl-4-hydroxyphenylpropionic acid and pentaerythritol; sodium cyanoborohydride; L-proline; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2019.130883
upstream raw materials:

phenylsulfonylnitromethane

Octanal

Downstream raw materials:

1-nitrononane

nonan-1-al

nonanoic acid

nonanamide

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