6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione

Base Information

• Chemical Name: 6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione
• CAS No.: 1145713-13-8
• Molecular Formula: C₃₅H₂₆Cl₂N₄O₂S
• Molecular Weight: 637.589

Synonyms:

Chemical Property of 6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione

Chemical Property:

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Safty Information:

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Useful:

Technology Process of 6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione

There total 2 articles about 6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(chlorophenyl)-10-(4-chlorophenylmethylene)-7,8,9,10-tetrahydrothiazolo[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione (1145713-15-0) + 4-dimethylamino-benzaldehyde (100-10-7) → 6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione (1145713-13-8)

Guidance literature:

6-(chlorophenyl)-10-(4-chlorophenylmethylene)-7,8,9,10-tetrahydrothiazolo[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione; 4-dimethylamino-benzaldehyde; With sodium acetate; acetic anhydride; acetic acid; for 5h; Reflux;

With water; at 20 ℃; Cooling;

DOI:10.1016/j.ejmech.2008.03.022

Reference yield:

9-(4-chlorophenylmethylene)-5-(4-chlorophenyl)-2-thioxo-2,3,6,7,8,9-hexahydropyrimido[4,5-b]quinolin-4(1H)-one (1027003-73-1) + chloroacetic acid (79-11-8) + 4-dimethylamino-benzaldehyde (100-10-7) → 6-(4-chlorophenyl)-10-(4-chlorophenylmethylene)-2-(4-N,N-dimethyl-aminophenylmethylene)-7,8,9,10-tetrahydrothiazolo-[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione (1145713-13-8)

Guidance literature:

9-(4-chlorophenylmethylene)-5-(4-chlorophenyl)-2-thioxo-2,3,6,7,8,9-hexahydropyrimido[4,5-b]quinolin-4(1H)-one; chloroacetic acid; 4-dimethylamino-benzaldehyde; With sodium acetate; acetic anhydride; acetic acid; for 15h; Reflux;

With water; Cooling;

DOI:10.1016/j.ejmech.2008.03.022

upstream raw materials:

9-(4-chlorophenylmethylene)-5-(4-chlorophenyl)-2-thioxo-2,3,6,7,8,9-hexahydropyrimido[4,5-b]quinolin-4(1H)-one

chloroacetic acid

4-dimethylamino-benzaldehyde

6-(chlorophenyl)-10-(4-chlorophenylmethylene)-7,8,9,10-tetrahydrothiazolo[3',2':1,2]pyrimido[4,5-b]quinoline-3,5-dione

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