bis{2-(phenylazo)pyridine}copper(I) perchlorate

Base Information

Chemical Name:bis{2-(phenylazo)pyridine}copper(I) perchlorate
CAS No.:84647-95-0
Molecular Formula:C₂₂H₁₈CuN₆*ClO₄
Molecular Weight:529.422
Hs Code.:

Synonyms:

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Chemical Property of bis{2-(phenylazo)pyridine}copper(I) perchlorate

Chemical Property:

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Technology Process of bis{2-(phenylazo)pyridine}copper(I) perchlorate

There total 3 articles about bis{2-(phenylazo)pyridine}copper(I) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84647-93-8
bis(2-(phenylazo)pyridine)copper(II) diperchlorate

: 84647-95-0
bis{2-(phenylazo)pyridine}copper(I) perchlorate

Guidance literature:: In solid; slowly converted to the copper(I) form in the presence of moisture evenin the solid state;

Reference yield:

: copper(II) perchlorate hexahydrate

: 2569-57-5
2-(phenylazo)pyridine

: 84647-95-0
bis{2-(phenylazo)pyridine}copper(I) perchlorate

Guidance literature:: In methanol; water; 2-(phenylazo)pyridine added dropwise to soln. Cu(ClO4)2*6H2O in 2:1 methanol-water and mixt. boiled under reflux for 48 h; soln. evapd. on water bath, residue washed with water, dissolved in methanol and left for crystn., crystals filtered, dried under vac. over P4O10;

Reference yield:

: 2569-57-5
2-(phenylazo)pyridine

: 14057-91-1
tetrakis(acetonitrile)copper(I) perchlorate

: 84647-95-0
bis{2-(phenylazo)pyridine}copper(I) perchlorate

Guidance literature:: In acetonitrile; under N2 atm. 2-(phenylazo)pyridine added dropwise to soln.(Cu(CH3CN)4)(ClO4) in dry acetonitrile with stirring and stirred at room temp. for 30 min; crystals filtered off and recrystd. from methanol; elem. anal.;