6-(2-Aminophenyl)hexanoic acid

Base Information

Chemical Name:6-(2-Aminophenyl)hexanoic acid
CAS No.:100369-74-2
Molecular Formula:C₁₂H₁₇NO₂
Molecular Weight:207.272
Hs Code.:

Synonyms:

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Chemical Property of 6-(2-Aminophenyl)hexanoic acid

Chemical Property:

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Technology Process of 6-(2-Aminophenyl)hexanoic acid

There total 4 articles about 6-(2-Aminophenyl)hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(dibenzylamino)phenyl trifluoromethanesulfonate

: 100369-74-2
6-(2-Aminophenyl)hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: lithium chloride; magnesium; zinc(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-(dibutylphosphanyl)-1-phenylpyrrole / tetrahydrofuran / 16 h / 60 °C / Inert atmosphere; Glovebox; Sealed tube

2: hydrogen / ethanol / 20 °C / 760.05 Torr / Inert atmosphere

3: lithium hydroxide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-(dibutylphosphanyl)-1-phenylpyrrole; hydrogen; magnesium; lithium chloride; zinc(II) chloride; lithium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1002/anie.201608535

Reference yield:

: 2-(dibenzylamino)phenol

: 100369-74-2
6-(2-Aminophenyl)hexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: lithium chloride; magnesium; zinc(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-(dibutylphosphanyl)-1-phenylpyrrole / tetrahydrofuran / 16 h / 60 °C / Inert atmosphere; Glovebox; Sealed tube

3: hydrogen / ethanol / 20 °C / 760.05 Torr / Inert atmosphere

4: lithium hydroxide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

With pyridine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-(dibutylphosphanyl)-1-phenylpyrrole; hydrogen; magnesium; lithium chloride; zinc(II) chloride; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/anie.201608535

Reference yield:

: 823-22-3,26991-67-3
5-hexanolide

: 100369-74-2
6-(2-Aminophenyl)hexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; hydrogen bromide / 4 h / 75 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: lithium chloride; magnesium; zinc(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-(dibutylphosphanyl)-1-phenylpyrrole / tetrahydrofuran / 16 h / 60 °C / Inert atmosphere; Glovebox; Sealed tube

3.1: hydrogen / ethanol / 20 °C / 760.05 Torr / Inert atmosphere

4.1: lithium hydroxide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-(dibutylphosphanyl)-1-phenylpyrrole; hydrogen bromide; hydrogen; magnesium; acetic acid; lithium chloride; zinc(II) chloride; lithium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1002/anie.201608535