(ferrocenylmethyl)[2,2-dimethyl-2-hydroxyethyl]ammonium picrate

Base Information

• Chemical Name: (ferrocenylmethyl)[2,2-dimethyl-2-hydroxyethyl]ammonium picrate
• CAS No.: 1031307-66-0
• Molecular Formula: C₆H₃N₃O₇*C₁₅H₂₁FeNO
• Molecular Weight: 516.291
• Mol file: 1031307-66-0.mol

Synonyms:

Chemical Property of (ferrocenylmethyl)[2,2-dimethyl-2-hydroxyethyl]ammonium picrate

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of (ferrocenylmethyl)[2,2-dimethyl-2-hydroxyethyl]ammonium picrate

There total 1 articles about (ferrocenylmethyl)[2,2-dimethyl-2-hydroxyethyl]ammonium picrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

2-(ferrocenylmethyl)amino-2-methyl-propan-1-ol (680622-40-6) + 2,4,6-Trinitrophenol (88-89-1) → (ferrocenylmethyl)[2,2-dimethyl-2-hydroxyethyl]ammonium picrate (1031307-66-0)

Guidance literature:

In ethyl acetate; picric acid dissolved in min. vol. of ethyl acetate; added to concd. soln. of Fe complex in ethyl acetate; layered with hexane; crystd. at 4°C by diffusion for several d; ppt. isolated by suction; washed with hexane; dried under reduced pressure; elem. anal.;

DOI:10.1016/j.jorganchem.2008.01.036

upstream raw materials:

2-(ferrocenylmethyl)amino-2-methyl-propan-1-ol

2,4,6-Trinitrophenol