((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

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Chemical Name:((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene
CAS No.:1242061-22-8
Molecular Formula:C₃₆H₃₈O
Molecular Weight:486.697
Hs Code.:

Synonyms:

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Chemical Property of ((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

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Technology Process of ((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

There total 2 articles about ((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4R,6R)-methyl 2,4,6-trimethyl-7-(trityloxy)hept-2-enoate

: ((((2R,4R,5E,7Z)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

: 1242061-22-8
((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 20 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; lithium hexamethyldisilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; 1.1: |Wittig Olefination / 2.1: |Wittig Olefination / 3.2: |Julia-Kocienski Olefination;
DOI:10.1002/chem.201201585

Reference yield:

: 1242061-31-9
(4R,6R,E)-2,4,6-trimethyl-7-(trityloxy)hept-2-en-1-ol

: ((((2R,4R,5E,7Z)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

: 1242061-22-8
((((2R,4R,5E,7E)-2,4,6-trimethyl-8-phenylocta-5,7-dien-1-yl)oxy)methanetriyl)tribenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With lithium hexamethyldisilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; 1.1: |Wittig Olefination / 2.2: |Julia-Kocienski Olefination;
DOI:10.1002/chem.201201585